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Nitrogen generators

 

In today’s modern analytical laboratory compressed air is required for a wide range of different uses.

 

Nitrogen purposes

Nitrogen is used for two purposes in the separation of molecules.

The first purpose is called curtain gas. When a sample enters the instrument, it is first atomized by a dry gas and sprayed into the inlet of the MS-instrument. The nitrogen forms a curtain of gas behind the inlet of the instrument. In order to separate and analyze the sample, this must be under vacuum. The curtain prevents air from entering along with the examined sample.

The second purpose of nitrogen is called collision gas. After ions enter the MS-instrument, they are accelerated and made to collide with the second reservoir of nitrogen - collision gas. The purpose of the collision gas is to break up the molecules of the sample to determine their composition.

 

Nitrogen generator technologies

In order to produce nitrogen, the generator requires compressed air. Atmospheric air contains roughly 78% nitrogen, 21% oxygen, 0.9% argon and the balance is other gasses. The compressed air which reaches the nitrogen generator has the same composition. To produce a specific gas, the generator needs to separate the required gas molecules in the compressed air, and two different technologies of separation are used to produce nitrogen: PSA (Pressure Swing Adsorption) and membrane technology.

PSA is a filtration technology, which utilizes carbon molecular sieve (CMS) to separate the nitrogen from the other gasses. The PSA system normally contains two beds of CMS, which simultaneously either receives compressed air or leads the adsorbed gasses out of the PSA-beds.

Membrane technology is based on a bundle of small individual hollow fibres. Each fibre has circular cross-sections and a uniform bore through its center. When the compressed air under high pressure enters the surface area, the gasses inside the air are divided up and forced into each fibre. Oxygen and water vapour are considered gasses, which quickly run through the fibres and even permeate the membranes. This allows the final gas - nitrogen - to flow through the fibre bores as the product steam.

Due to the small size of the fibres, a high number may be placed into a limited space and provide an extremely large membrane surface area, allowing for a high nitrogen output.

In comparison, the membrane system requires higher airflow than PSA in order to produce the equivalent amount of nitrogen.

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